NSC 84180
3-Chloropropionyl chloride
CAS: 625-36-5
Molecular Formula: C3H4Cl2O
NSC 84180 - Names and Identifiers
NSC 84180 - Physico-chemical Properties
| Molecular Formula | C3H4Cl2O |
| Molar Mass | 126.97 |
| Density | 1.33g/mLat 25°C(lit.) |
| Melting Point | -32 °C |
| Boling Point | 143-145°C(lit.) |
| Flash Point | 146°F |
| Water Solubility | reacts |
| Solubility | Chloroform, Ethyl Acetate |
| Vapor Presure | 10.0 hPa |
| Appearance | liquid |
| Color | red-brown |
| BRN | 635814 |
| PH | <7 (H2O) |
| Storage Condition | Flammables area |
| Stability | Moisture Sensitive |
| Sensitive | Moisture Sensitive |
| Explosive Limit | 8.8-20.2%(V) |
| Refractive Index | n20/D 1.457(lit.) |
| Physical and Chemical Properties | Appearance colorless transparent liquid corrosion product |
| Use | Used as an intermediate in organic synthesis |
NSC 84180 - Risk and Safety
| Hazard Symbols | T+ - Very toxic |
| Risk Codes | R14 - Reacts violently with water R22 - Harmful if swallowed R26 - Very Toxic by inhalation R34 - Causes burns R35 - Causes severe burns R10 - Flammable |
| Safety Description | S23 - Do not breathe vapour. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S38 - In case of insufficient ventilation, wear suitable respiratory equipment. S16 - Keep away from sources of ignition. S8 - Keep container dry. |
| UN IDs | UN 3390 6.1/PG 1 |
| WGK Germany | 1 |
| RTECS | UC3934000 |
| FLUKA BRAND F CODES | 21 |
| TSCA | Yes |
| HS Code | 29159080 |
| Hazard Class | 6.1 |
| Packing Group | I |
NSC 84180 - Upstream Downstream Industry
| Raw Materials | 3-Chloropropionic acid |
NSC 84180 - Reference Information
| NIST chemical information | information provided by: webbook.nist.gov (external link) |
| EPA chemical substance information | information provided by: ofmpeb.epa.gov (external link) |
| Use | for organic synthesis. used as intermediate in organic synthesis |
| production method | is obtained by reacting propionic acid with sulfuryl chloride and thionyl chloride. 59.2G of propionic acid, 54.0G of sulfuryl chloride and 61.6g of carbon tetrachloride were mixed, and 0.5g of benzoyl peroxide was added. Reflux was protected from light for 1.5h until there was no further gas evolution. Additional excess thionyl chloride 190.4g was added and refluxed for 4H. The solvent is then evaporated off at atmospheric pressure and the excess of thionyl chloride and propionyl chloride. The remainder was fractionated under reduced pressure, and 2-chloropropionyl chloride was collected as the 51-54 ℃(13.3kPa) fraction, and 3-chloropropionyl chloride was collected as the 81-84 ℃(13.3kPa) fraction, which accounted for 45% and 55%, respectively, the overall yield was 75%. |
Last Update：2024-04-09 02:00:10
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View History
Raw Materials for NSC 84180